• Isithando somlilo

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Ukukhulisa Ubude Besikhathi Sokuphila Kwezinto Ezibethelwa Nge-Graphite: Imiyalo Yokusebenza

I-Crucible Yokuncibilikisa Ithusi

Ekuphishekeleni ukukhulisa ubude bempilo kanye nokusebenzisa izici zeama-graphite crucibles, imboni yethu yenze ucwaningo olunzulu nokuhlola ekukhiqizeni nasekusebenzeni kwayo. Nansi imiyalo yokusebenza yezinsimbi ze-graphite:

Izinyathelo zokuphepha ezikhethekile ze-high-purity graphite crucibles:

Gwema ukushayisana kwemishini futhi ungawisi noma ushaye i-crucible usuka phezulu. Futhi gcina yomile futhi kude ifomu umswakama. Ungawathinti amanzi ngemva kokuba esebasiwe futhi omisiwe.

Uma usebenzisa, gwema ukuqondisa ilangabi ngqo phansi kwe-crucible. Ukuchayeka elangabini eliqondile kungashiya amamaki amnyama abalulekile.

Ngemva kokuvala isithando somlilo, susa noma iyiphi i-aluminiyamu esele noma impahla yethusi ku-crucible futhi ugweme ukushiya noma iyiphi insalela.

Sebenzisa izinto ezine-asidi (ezifana nokuguquguquka) ngokulingene ukuze uvimbele ukugqwala nokuqhekeka kwe-crucible.

Uma wengeza izinto, gwema ukushaya i-crucible futhi uyeke ukusebenzisa amandla omshini.

Ukugcinwa nokudluliswa kwama-graphite crucibles:

I-high-purity graphite crucibles iyazwela emanzini, ngakho-ke kufanele ivikelwe ekumswakama nokuchayeka kwamanzi.

Naka ukugwema ukulimala kwendawo. Ungabeki i-crucible ngqo phansi; esikhundleni salokho, sebenzisa i-pallet noma ibhodi lesitaki.

Uma uhambisa i-crucible, gwema ukuyigingqa ibhekise eceleni phansi. Uma idinga ukuphendukiswa iqonde phezulu, beka ikhadibhodi eliwugqinsi noma indwangu phansi ukuze uvimbele imihuzuko noma imihuzuko phansi.

Ngesikhathi sokudlulisa, qaphela ngokukhethekile ukuthi ungawisi noma ushaye i-crucible.

Ukufakwa kwezinsimbi ze-graphite:

I-crucible stand (iplatifomu e-crucible) kufanele ibe nobubanzi obufanayo noma obukhudlwana njengendawo engezansi ye-crucible. Ubude beplatifomu kufanele bube phezulu kunombobo welangabi ukuze kuvinjwe ilangabi ukuthi lifinyelele ku-crucible ngokuqondile.

Uma usebenzisa izitini eziphikisayo endaweni yesikhulumi, izitini eziyindilinga zikhethwa, futhi kufanele zibe flat ngaphandle kokugoba. Gwema ukusebenzisa izitini eziyingxenye noma ezingalingani, futhi kunconywa ukusebenzisa amapulatifomu e-graphite angenisiwe.

Beka indawo yokumisa ama-crucible phakathi nendawo yokuncibilika noma ukucwiliswa, bese usebenzisa impushana ye-carbon, i-rice husk ash, noma ukotini ophikisayo njengomcamelo ukuze uvimbele ukuthi i-crucible inganamatheli esitendini. Ngemuva kokubeka i-crucible, qiniseka ukuthi ilinganisiwe (usebenzisa izinga lomoya).

Khetha izinsimbi ezilinganayo ezihambisana nesithando somlilo, futhi ugcine igebe elifanele (okungenani (okungenani (40mm)) phakathi kwe-crucible nodonga lwesithando somlilo.

Uma usebenzisa i-crucible ene-spout, shiya isikhala esilinganiselwa ku-30-50mm phakathi kwe-spout nesitini esiphikisayo ngezansi. Ungabeki lutho ngaphansi, futhi sebenzisa ukotini ophikisayo ukwenza bushelelezi ukuxhumana phakathi kwe-spout nodonga lwesithando somlilo. Udonga lwesithando somlilo kufanele lube nezitini eziqinile eziphikisayo (amaphuzu amathathu), kanye nekhadibhodi likathayela cishe u-3mm ubukhulu kufanele libekwe ngaphansi kwe-crucible ukuvumela ukunwetshwa okushisayo ngemva kokushisa.

Ukushisa kuqala nokomiswa kwezinsimbi ze-graphite:

Shisisa i-crucible eduze kwesithando somlilo samafutha amahora angu-4-5 ngaphambi kokusetshenziswa ukuze usize ekususeni umswakama endaweni ye-crucible.

Ezitsheni ezintsha, faka amalahle noma ukhuni ngaphakathi kwe-crucible bese uyishisa cishe amahora amane ukuze usize ukususa umswakama.

Izikhathi zokushisisa ezinconyiwe ze-crucible entsha zimi kanje:

0℃ ukuya ku-200℃: Khulisa kancane izinga lokushisa ngaphezu kwamahora angu-4.

Ezithandweni zikawoyela: Khulisa izinga lokushisa kancane kancane ihora elingu-1, lisuka ku-0℃ liye ku-300 ℃, futhi lidinga amahora angu-4 ukusuka ku-200℃ liye ku-300℃,

Ezithandweni zikagesi: dinga amahora ama-4 wokushisisa ukusuka ku-300 ℃ kuye ku-800 ℃, bese amahora ama-4 ukusuka ku-300 ℃ kuye ku-400 ℃. kusuka ku-400 ℃ kuya ku-600 ℃, khulisa izinga lokushisa ngokushesha futhi ugcine amahora ama-2.

Ngemva kokuvala isithando somlilo, izikhathi ezinconyiwe zokushisisa kabusha zimi kanje:

Okwezithando zikawoyela nezikagesi: Kudingeka ihora elingu-1 isikhathi sokushisisa ukusuka ku-0℃ ukuya ku-300℃. Udinga amahora angu-4 wokushisisa ukusuka ku-300℃ ukuya ku-600℃. Khulisa ngokushesha izinga lokushisa liye ezingeni olifunayo.

Izinto zokushaja:

Uma usebenzisa i-high-purity graphite crucibles, qala ngokungeza izinto ezincane zamakhona ngaphambi kokwengeza izingcezu ezinkulu. Sebenzisa izindlawu ukubeka ngokucophelela nangokuthula izinto ku-crucible. Gwema ukulayisha ngokweqile i-crucible ukuze uvimbele ukuthi ingaphuki.

Ezithandweni zikawoyela, izinto zokwakha zingangezwa ngemva kokufinyelela ku-300 ℃.

Okwezithando zikagesi:

Ukusuka ku-200 ℃ kuya ku-300 ℃, qala ukungeza izinto ezincane. Kusukela ku-400℃ kuye phambili, kancane kancane engeza izinto ezinkulu. Uma ungeza izinto ngesikhathi sokukhiqiza okuqhubekayo, gwema ukuzifaka endaweni efanayo ukuze uvimbele i-oxidation emlonyeni we-crucible.

Ukuze uthole izithando zokushisa zikagesi, shisa kuqala ku-500 ℃ ngaphambi kokuthela i-aluminium encibilikayo.

Izinyathelo zokuqapha ngesikhathi sokusetshenziswa kwe-graphite crucibles:

Bamba izinto ngokunakekela uma uzingeza ku-crucible, ugwema ukubeka ngamandla ukuze uvimbele ukulimaza i-crucible.

Kuma-crucible asetshenziswa ngokuqhubekayo amahora angama-24, impilo yawo inganwetshwa. Ekupheleni kosuku lomsebenzi kanye nokuvalwa kwesithando somlilo, izinto ezincibilikisiwe ku-crucible kufanele zisuswe ukuze kuvinjelwe ukuqina nokwanda okulandelayo, okungaholela ekushintshashintsheni kwe-crucible noma ukuphuka.

Uma usebenzisa izinto ezincibilikayo (ezifana ne-FLLUX kuma-alloys e-aluminium noma i-borax kuma-alloys ethusi), zisebenzise kancane ukuze ugweme ukugqwala kwezindonga ezibohlayo. Engeza ama-agent lapho ukuncibilika kwe-aluminium sekukude nemizuzu engu-8 ukuthi igcwale, inyakaze ngobumnene ukuze ibavimbele ekubambeleleni ezindongeni ezibhobozayo.

Qaphela: Uma i-ejenti encibilikayo iqukethe ngaphezu kuka-10% we-sodium (Na) okuqukethwe, kudingeka i-crucible ekhethekile eyenziwe ngezinto ezithile.

Ekupheleni kosuku ngalunye lomsebenzi, ngenkathi i-crucible isashisa, susa ngokushesha noma iyiphi insimbi enamathela ezindongeni ezihlabayo ukuze uvimbele izinsalela eziningi, ezingase zithinte ukudluliswa kokushisa nokwelula isikhathi sokuhlakazeka, okubangela ukwanda okushisayo kanye nokuphuka okungase kube khona kwe-crucible.

Kunconywa ukuthi uhlole isimo se-crucible cishe njalo ezinyangeni ezimbili ukuze uthole ama-alloys e-aluminium (masonto onke ama-alloys ethusi). Hlola indawo yangaphandle bese uhlanza igumbi lesithando somlilo. Ukwengeza, zungezisa i-crucible ukuze uqinisekise ukuguga, okusiza ukunweba ubude besikhathi sempilo ye-high-purity graphite crucibles.

Ngokulandela le miyalo yokusebenza, abasebenzisi bangakwazi ukukhulisa isikhathi sokuphila nokusebenza kahle kwe-graphite crucibles yabo, baqinisekise ukusebenza okuhle ezinhlelweni ezihlukahlukene.


Isikhathi sokuthumela: Jul-10-2023