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Indlela yokukhiqiza ama-graphite crucibles

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I-graphite crucibleiwumkhiqizo okhethekile odlala indima ebalulekile ekucwengisweni kwegolide, isiliva, ithusi nezinye izinsimbi eziyigugu. Nakuba abantu abaningi bengase bangazijwayele, ukukhiqizwa kwezinsimbi ze-graphite kuhilela izigaba eziningana eziyinkimbinkimbi ukuze kuqinisekiswe ikhwalithi ephakeme namandla omshini womkhiqizo wokugcina. Kulesi sihloko, sizocubungula imininingwane yesiteji ngasinye esibandakanyekayo enqubweni yokukhiqiza i-graphite crucible.

Izigaba zokuqala zokukhiqiza ama-graphite crucibles zibandakanya inqubo yokomisa. Ngemva kokwakhiwa kwe-crucible kanye nezingxenye zayo ezilengayo ezisekelayo, ziyahlolwa ngokuvumelana nezindinganiso zomkhiqizo osuphelile. Lokhu kuhlola kuqinisekisa ukuthi abantu abaqeqeshiwe kuphela badlulela ezigabeni ezilandelayo. Ngemuva kokuhlunga, zenza inqubo yokucwebezela, lapho i-crucible surface imbozwe nge-glaze. Lolu ngqimba olucwebezelayo lufeza izinjongo ezimbalwa, okuhlanganisa ukukhulisa ukuminyana namandla emishini ye-crucible, ekugcineni ithuthukise ikhwalithi yayo yonke.

Isiteji sokudubula siyingxenye ebalulekile yenqubo yokukhiqiza. Kuhilela ukufaka i-graphite crucible emazingeni aphezulu okushisa kuhhavini, ngaleyo ndlela kuqiniswe ukwakheka kwe-crucible. Le nqubo ibalulekile ukuze kuqinisekiswe ukuqina nokuthembeka kwe-crucible phakathi nenqubo yokucwenga. Isimiso sokudubula singahlukaniswa sibe izigaba ezine ezihlukene ukuze uqonde kangcono izinguquko ezenzeka esakhiweni se-crucible phakathi nale nqubo.

Isigaba sokuqala yisiteji sokushisa nokudubula, futhi izinga lokushisa kuhhavini ligcinwa cishe ku-100 kuya ku-300 ° C. Kulesi sigaba, umswakama osele ku-crucible uyasuswa kancane kancane. Vula i-skylight ye-kiln futhi wehlise izinga lokushisa ukuze uvimbele ukushintsha okungazelelwe kwezinga lokushisa. Ukulawula izinga lokushisa kubalulekile kulesi sigaba, njengoba umswakama omningi oyinsalela ungabangela ukuqhekeka kwe-crucible noma ngisho nokuqhuma.

Isigaba sesibili yisigaba sokudubula esisezingeni eliphansi, esinezinga lokushisa elingu-400 kuya ku-600°C. Njengoba iziko liqhubeka nokushisa, amanzi abophekile ngaphakathi kwe-crucible aqala ukuphuka futhi ahwamuke. Izingxenye eziyinhloko i-A12O3 ne-SiO2, ezaziboshwe ngaphambili obumba, ziqala ukuba khona esimweni esikhululekile. Kodwa-ke, kufanele kuqashelwe ukuthi ungqimba lwe-glaze ebusweni be-crucible alukakancibiliki okwamanje. Ukuze uvimbele noma yiziphi izimanga, izinga lokushisa kufanele lihlale linensa futhi lizinzile. Ukushisa okusheshayo nokungalingani kungabangela ukuthi i-crucible iqhekeke noma iwe, ibeke engozini ubuqotho bayo.

Ukungena esigabeni sesithathu, izinga lokushisa eliphakathi nendawo ngokuvamile livela phakathi kuka-700 no-900°C. Kulesi sigaba, i-Al2O3 e-amorphous obumba iguqulwa kancane ukuze yakhe i-Y-type crystalline Al2O3. Lolu shintsho luthuthukisa futhi ubuqotho besakhiwo se-crucible. Kubalulekile ukugcina izinga lokushisa elinembile ngalesi sikhathi ukugwema noma yimiphi imiphumela engathandeki.

Isigaba sokugcina yisigaba sokudubula esisezingeni eliphezulu, esinezinga lokushisa elingaphezu kuka-1000°C. Kuleli qophelo, ungqimba olucwebezelayo lugcina luncibilika, luqinisekise ukuthi indawo ye-crucible ibushelelezi futhi ivalekile. Amazinga okushisa aphezulu aphinde anikele ekuthuthukisweni okuphelele kwamandla emishini ye-crucible kanye nokuqina.

Sekukonke, inqubo yokukhiqiza izinsimbi ze-graphite ihilela izigaba ezimbalwa zokucophelela. Ukusuka ekomisweni nasekuhloleni umkhiqizo osuphelile ukuya ekucwebezeni nasekudubuleni, isinyathelo ngasinye sibalulekile ekuqinisekiseni ikhwalithi nokuthembeka kwe-crucible yokugcina ye-graphite. Ukunamathela ezilinganisweni zokulawula izinga lokushisa nokugcina amazinga okushisa afanele kubalulekile ekuvimbeleni noma yiziphi izinkinga ezingase zibe khona noma izingozi. Umphumela uba i-graphite crucible yekhwalithi ephezulu ekwazi ukumelana nenqubo yokucwenga ngokuqinile yezinsimbi eziyigugu.


Isikhathi sokuthumela: Nov-29-2023